Considerations in conducting adhesion experiments via nanoindentation

dc.contributor.advisorLiechti, K. M.
dc.creatorMartinez, Kevin Michael
dc.creator.orcid0000-0003-3816-9859
dc.date.accessioned2018-08-07T17:30:43Z
dc.date.available2018-08-07T17:30:43Z
dc.date.created2017-12
dc.date.issued2017-12-08
dc.date.submittedDecember 2017
dc.date.updated2018-08-07T17:30:43Z
dc.description.abstractRecent attempts to commercialize graphene-based technology for flexible electronics applications have largely failed due to a lack of scalable, cost effective graphene transfer options. Dry graphene R2R transfer processes have numerous advantages over wet processes, but their development requires further characterization of the graphene-substrate interfaces. In support of this initiative, a displacement-controlled nanoindenter experimental protocol was developed for characterizing adhesion interactions between a diamond probe and specimen substrate surface. This protocol was used to characterize probe interactions with quartz, graphite, and silicon samples in ambient and nitrogen environments. Available literature data for diamond probe-silicon interactions correspond well to our work. However, persistent adhesive snap-behavior due to motor control deficiency in the selected device significantly reduced the utility of this technique. Resolution of full interaction behavior is severely impacted and is reduced to the order of 5 nm from the stated transducer capability of 0.4 nm.
dc.description.departmentElectrical and Computer Engineering
dc.format.mimetypeapplication/pdf
dc.identifierdoi:10.15781/T25718599
dc.identifier.urihttp://hdl.handle.net/2152/65987
dc.language.isoen
dc.subjectNanoindentation
dc.subjectGraphene
dc.subjectAdhesion
dc.subjectHysitron
dc.subjectGraphene transfer
dc.subjectGraphene-substrate interfaces
dc.subjectGraphene-based technology
dc.subjectAdhesion interactions
dc.subjectDiamond probe-silicon interactions
dc.subjectAdhesive snap-behavior
dc.titleConsiderations in conducting adhesion experiments via nanoindentation
dc.typeThesis
dc.type.materialtext
thesis.degree.departmentEngineering Mechanics
thesis.degree.disciplineEngineering Mechanics
thesis.degree.grantorThe University of Texas at Austin
thesis.degree.levelMasters
thesis.degree.nameMaster of Science in Engineering

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