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Detection of unstable intermediates and mechanistic studies in multisteps, two-electron transfer reactions by cyclic voltammetry and scanning electrochemical microscopy
(2014-05)
Unstable Sn(III) intermediates generated in the Sn(IV)/Sn(II) redox reaction in 2 M HBr + 4 M NaBr media were detected by scanning electrochemical microscopy (SECM) and cyclic voltammetry (CV). In CV, the underpotential ...